Dayton Chapter of ASM International

 

 Dayton Chapter Joint Meeting with Cincinnati ASM and Dayton AWS

Thursday, January 11, 2007

 

3D Characterization of the Structure and Crystallography of Aerospace Materials using a Dual Beam FIB-SEM

 

Speaker

Dr. Michael D. Uchic

Air Force Research Laboratory

Dayton, OH

 

 

 

                                                                                                                                                   Location:

5:30 p.m.             Social                                                                                                    Chantrells Restaurant

6:30 p.m.             Dinner ($20.00, Students: FREE)                                                              20 Commercial Way

7:30 p.m.             Program                                                                                                      Springboro, Ohio

                                                                                                                                               937-743-6073

For Reservations:                                                                                                              Menu:  

                     Call Chuck Woods 937-236-8315                                                                   salmon, onion rib eye

                     E-mail: cwoods@globalms.com                                                                     Sautee Zucchini, Squash

                     On-line: http://www.asm-dayton.org                                                          Wild Rice Pilaf

                     By 3:00 p.m. Wednesday, January 10, 2007                                                       7-layer salad, Appetizer

                                                                                                                                 Rolls, Seasonal pies and Cakes, Beverage

 

ABSTRACT

 

The Dual Beam Focused Ion Beam (FIB)-Scanning Electron Microscope (SEM) has proved to be a powerful instrument for characterizing the microstructure and crystallography of aerospace materials in 3D. The DB FIB-SEM is capable of in-situ, high fidelity serial sectioning, where the serial sectioning slice thickness can be ~25 nanometers, and the interrogated volume can be as large as 50 x 50 x 50 micrometers in dimension. Custom scripting routines have been developed at AFRL to automate the serial sectioning experiments. Notably, the scripting program is designed to control the acquisition of a variety of characterization data from each sectioned surface. This data includes electron images, ion images, crystallographic orientation maps (EBSD), and chemistry maps (EDS). This talk will focus on the application of the Dual Beam microscope to characterize Ni base superalloys in 3D, but examples from other alloy systems will also be shown.  

 

 

SPEAKER BIO

 

Michael D. Uchic, Air Force Research Laboratory

Michael D. Uchic is a materials research engineer in the Metals Development Group of the Air Force Research Laboratory, Materials & Manufacturing Directorate. He received his Ph.D. from Stanford University, and for his thesis topic he characterized the low-temperature mechanical properties of the intermetallic alloy Ni3Al.